Amino acid separation by preparative temperature-swing chromatography with flow reversal
Identifieur interne : 002363 ( Main/Exploration ); précédent : 002362; suivant : 002364Amino acid separation by preparative temperature-swing chromatography with flow reversal
Auteurs : Gabor Simon [France, Hongrie] ; Laszlo Hanak [Hongrie] ; Georges Grévillot [France] ; Tibor Szanya [Hongrie] ; Gyula Marton [Hongrie]Source :
- Journal of Chromatography A [ 0021-9673 ] ; 1996.
English descriptors
- KwdEn :
- Adsorbent, Adsorption, Adsorption isotherms, Aiche, Amino, Amino acid, Amino acid concentration, Amino acid concentrations, Amino acid uptake, Amino acids, Arginine, Arginine concentration, Batch rectification, Bottom reservoir, Bottom reservoir concentration, Breakthrough volume, Chromatogr, Cold flow, Cold isotherms, Cold temperature, Different degrees, Different temperatures, Effluent volume, Experimental conditions, Histidine, Histidine concentration, Initial concentrations, Isotherm, Lysine, Lysine concentration, Lysine histidine, Lysine histidine arginine, Parametric, Possible ways, Previous case, Rectification, Reflux, Reflux ratio, Reservoir, Reservoir concentration, Schematic diagram, Special type, Temperature change, Temperature dependence, Traditional batch.
- Teeft :
- Adsorbent, Adsorption, Adsorption isotherms, Aiche, Amino, Amino acid, Amino acid concentration, Amino acid concentrations, Amino acid uptake, Amino acids, Arginine, Arginine concentration, Batch rectification, Bottom reservoir, Bottom reservoir concentration, Breakthrough volume, Chromatogr, Cold flow, Cold isotherms, Cold temperature, Different degrees, Different temperatures, Effluent volume, Experimental conditions, Histidine, Histidine concentration, Initial concentrations, Isotherm, Lysine, Lysine concentration, Lysine histidine, Lysine histidine arginine, Parametric, Possible ways, Previous case, Rectification, Reflux, Reflux ratio, Reservoir, Reservoir concentration, Schematic diagram, Special type, Temperature change, Temperature dependence, Traditional batch.
Abstract
Abstract: A special type of adsorptive parametric pumping called temperature-swing chromatography is experimentally investigated for a new application: the separation of amino acids. Experiments have been done with a mixture of arginine, histidine and lysine in acidic solution (HCl). A multicomponent equilibrium model has been used to simulate the experimental results and to investigate some possible ways to improve the separation. It is shown that it is possible to separate these amino acids, and the composition of the products strongly depends on the experimental conditions. Arginine with purity greater than 95% can be obtained by applying these methods.
Url:
DOI: 10.1016/0021-9673(95)01184-6
Affiliations:
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Le document en format XML
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<term>Amino acid</term>
<term>Amino acid concentration</term>
<term>Amino acid concentrations</term>
<term>Amino acid uptake</term>
<term>Amino acids</term>
<term>Arginine</term>
<term>Arginine concentration</term>
<term>Batch rectification</term>
<term>Bottom reservoir</term>
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<term>Cold temperature</term>
<term>Different degrees</term>
<term>Different temperatures</term>
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<term>Experimental conditions</term>
<term>Histidine</term>
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<term>Initial concentrations</term>
<term>Isotherm</term>
<term>Lysine</term>
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<term>Lysine histidine arginine</term>
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<term>Rectification</term>
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<term>Reservoir concentration</term>
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<term>Special type</term>
<term>Temperature change</term>
<term>Temperature dependence</term>
<term>Traditional batch</term>
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<term>Bottom reservoir</term>
<term>Bottom reservoir concentration</term>
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<term>Cold flow</term>
<term>Cold isotherms</term>
<term>Cold temperature</term>
<term>Different degrees</term>
<term>Different temperatures</term>
<term>Effluent volume</term>
<term>Experimental conditions</term>
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<term>Histidine concentration</term>
<term>Initial concentrations</term>
<term>Isotherm</term>
<term>Lysine</term>
<term>Lysine concentration</term>
<term>Lysine histidine</term>
<term>Lysine histidine arginine</term>
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<term>Possible ways</term>
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<term>Reservoir concentration</term>
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<front><div type="abstract" xml:lang="en">Abstract: A special type of adsorptive parametric pumping called temperature-swing chromatography is experimentally investigated for a new application: the separation of amino acids. Experiments have been done with a mixture of arginine, histidine and lysine in acidic solution (HCl). A multicomponent equilibrium model has been used to simulate the experimental results and to investigate some possible ways to improve the separation. It is shown that it is possible to separate these amino acids, and the composition of the products strongly depends on the experimental conditions. Arginine with purity greater than 95% can be obtained by applying these methods.</div>
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